Annexes
Annexe 1 : Diffractogrammes sur poudre totale
40000
Kaulinite F-k
Muscovite
07, P.
LUTENDELEII
Qua cif
10000
0
2-Theta - Scale
®LUTENDELEII -Fie: LUTENDELEII 1002.rew- Type: Locked
Coupled - Start 2.000 ° -End: 45.002 ° -Step: 0.021 °- Step
time:48. c- Tamp.: 25 °C (Roan) -Time Started:0 s-2-Theta: 2.000 ° -T
operations: Smooth 0150 I Background 0.000.0.0001 Background 0.000.0.0001
Import
LUTENDELEIII
50000 --
Quarte
Kaolinite
m
Muscovite
tAr
40000
C 30000
q -
U -
c
J
20000 --
10000
10
AT
20
Guethite
F-k
P-Zy
69
2-Theta - Scale
®LUTENDELEIu - 910: LUTENDELEIII 1007.raw -Type:
LOcked c0tlpied - Stont 2.000 ° - End: 45.002 ° - 510p: 0.021 °
- 51011 time: 40.5 -Tamp.:25 °C (R00m)- Una Stalled: 0 u - 2-Thata: 2.000
° Operations: Background 0.000.0.0001 Smooth 0.150 I Irryorl
QLUTENDELEIII - RIO: LUTENDELEIII_1007.ra0 -Type:
Locked Coupled - Start: 2.000 ° - End: 45.002 ° - 510p:
0.021 ° - Step tine: 40. S -Tamp.:25 °C (Room)- 1-000
Started: 0 u - 2-Theta: 2 000 ° -Operatians: Background 0000.0.000 1
Background 0000.0000!Smooth 01521 Import
NSAYA1 I
80000 --
50000 --
ammo
-
D
O 30000 --
J -
20000
10000
2-Theta - Scale
®NSAYAI I - RIB: NSAYA11_1003 saw -Type'. Locked Coupled -
Start: 2.000 ° - End: 45.002 ° - Slop: 0.021 ° - Step limo: 48.
e-Tamp.: 25 °C (Room) - Tim Started: 0 5 - 2-Theta: 2.000 ° - Theta:
1.00 Operations: Smooth 0.150 !Import
NSAYA1II
Quartz
30000 --o
0
U_ -
c
J
k.ulimite AT
Ta
·
10000
0
10
20 30
70
2-Theta - Scale
®NSAYA111 - File: 0SAYA111_1010.raw- Type: Locked Coupled -
Start 2.000 ° - CM: 45.002 ° - Stap: 0.021 ° - Stop ion: 48. 5
-Temp.: 25 °C (Room)-Time Started: 0 5 -2 Theta: 2.000 ° -Theta: 1.0
Operations: Smooth 0.1501 Background 00000X101 Import
71
NSAYA2II
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QUArt2
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Goethite
AT
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30000 --
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tn
D U
Ç2
J
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10000
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Knolinile
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10
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20
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30 40
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2-Theta - Scale
®NSAYA211 - File: NSAYA211_1001.raw - Typo: Locked Coupled -
Sun: 2.000 ° - Bud: 45.002 ° - Stop: 0.021 ° - Stop time: 48. s
- Temp.: 25 °C (Room)-Time Staltod: 0 5 - 2-moto: 2.000 ° -Theta: 1.0
Operations: Smooth 0.150 I Background 0.000.0.200 Import
C3CECOMAF
50000 --
Quartz
40000
Fk
s
51.
AT v
10000 --
Kaolinite
20000 --
C
ethite
Muscovite
10
2-Theta - Scale
®C3CECOMAF - File: C3CECOMAF_1009.row- Type: Lacked Coupled
- sun: 2.000 ° - End: 45.002 ° - Step: 0.021 ° - Step lima: 48.
s- Tamp.: 25 °C (Room) - Time Starred: 0 s- 2-Thola: 2.000 ° - Theta:
Operations. Smooth 0.1501 Background 0.000.0.200 Import
C3KIMBANGUIII
50000 0
U_
Ç 40000
3000
20000
Kaolinite
Muscovite
1000
Quart/
0
AT
2 10 20
la
Goethite
F-k
8
30 40
72
2-Theta - Scale
®C310M13ANGUIII - File: C3KIMBANGUIII_1006.raw- Typo: Lockod
Coupled - Start 2.00 ° - End: 45.002 ° - Stop: 0.021 ° - Stop
One: 48.5- Temp.: 25 °C (Roan) -Tirna
Slatted: 0 5- 2-Th41a: 2.00 ° -Th Operations:
Smooth 0.150 I Background 0.000..00 Irrpod
C3NSAYA1 I
2
20
10
30 40
3000 --
Gncthite
10000 --
2-Theta - Scale
QC3NSAYAI I - File: C3NSAYA11_1012. raw -Type'. Locked
Coupled - Start:2.00 ° - End: 45.002 ° - Slop: 0.021
° - Step limo: 48. 5-Tenlp.: 25 °C (Roan) - Tinto Started: 0
S-2-Thora: 2.000 ° - Thora: 1.00 Operations: Smooth 0.1501
Background 0.000..220 Import
73
C3NSAYA1II
Quartz
cici
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Kaolinite
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AT
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Hematite
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CO
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RO
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oi
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10000 --
30000 --
2 10
2-Theta - Scale
(c)C3NSAYA1111 - Fite: C3NSAYA1111 1004.raw - Type: Lacked
Coupled - Start: 2.000 ° - End: 45.002 ° - Stop: 0.021
° - Step time: 48. 5- Temp.: 25 °C (Room) - Trme Started: 0 5 -
2-Theta: 2.000 ° - Theta: 1. Operations: Smooth 0.150 I Background
0.0000.220 Import
C4 N SAYA 1 I I
Quart"
2
30000
10000 --
Kaolinite
·
0 JI.04V/4
Muscovite
of
10
2-Theta - Scale
®C4NSAYA111 - File: C4NSAYA111_1000.rew - Type: Locked
Coupled - Stan: 2.000 ° - Fard: 45.002 ° - Stop: 0.021 ° - Stop
lino: 48.5 - Temp.: 25 °C (Room)-Timo Monad: 0 5 - 2-Theta: 2.000 °
-Thoth: 1.0 Operations: Smooth 0.1501 Background 0.000,0.200 Import
74
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